Cycloheptanone → Cycloheptylidene(3-thienyl)acetonitrile

HRID 1814047Notes

Reaction equation

[S:1]1[CH:5]=[CH:4][C:3]([CH2:6][C:7]#[N:8])=[CH:2]1.[C:9]1(=O)[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1>>[C:9]1(=[C:6]([C:3]2[CH:4]=[CH:5][S:1][CH:2]=2)[C:7]#[N:8])[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

Participants

Reactant 2

HCID 10400Cycloheptanone

HCID 837303-Thienylacetonitrile

Product 1

HCID 22505729Cycloheptylidene(3-thienyl)acetonitrile

Procedure

The expected intermediate is obtained in the manner described in General Protocol A starting from 3-thienylacetonitrile and cycloheptanone.

Sources & evidence

ORD record: ord-61f95a1fe52441cdadc3e40d1cc3b8c1
Source dataset: uspto-grants-2005_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06875788B2

Reaction notes

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