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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1814136Generated: October 30, 2026

HCID 22504373, compound → HCID 22504424, compound

https://huagongshe.com/reaction/1814136

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22504373HCID 22504373—
CatalystHCID 178418406HCID 178418406—
SolventAcetoneHCID 180—
ProductHCID 22504424HCID 2250442449.3%

Reaction Conditions

Temperature22.5 °C

Reaction Steps

To a solution of the compound obtained in Example 34 (4) (123 mg) in acetone (40 ml), manganese dioxide (1.86 g) was added and the mixture was stirred at 15 to 30° C. for 1 hour. The reaction solution was filtered through Celite and concentrated under reduced pressure to obtain 60 mg (49.3%) of the desired product as a yellow powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06875770B2
Source datasetuspto-grants-2005_04
ORD IDord-16d6d0e8e25a4c15ac8f2df35cb14080
Source noteuspto-grants-2005_04