HuagongsheHuagongshe Chemistry Print Report · For research reference only
(6-Hydroxy-benzo[b]thiophen-3-yl)acetic acid methyl ester → HCID 69514708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (6-Hydroxy-benzo[b]thiophen-3-yl)acetic acid methyl ester | HCID 20765985 | — |
| Reactant | HCID 22504861 | HCID 22504861 | — |
| Product | HCID 69514708 | HCID 69514708 | — |
Reaction Steps
Compound 69C and Compound 5C were reacted in a manner analogous to Compound 59A to give {6-[2-(3-Fluoro-phenyl)-benzooxazol-5-ylmethoxy]-benzo[b]thiophen-3-yl}-acetic acid methyl ester. This was reacted in a manner analogous to Compound 59 to give the title product. 400 MHz 1H NMR (DMSO-d6) δ ppm 3.7 (s, 2H) 5.3 (s, 2H) 7.1 (dd, J=8.8, 2.4 Hz, 1H) 7.3 (s, 1H) 7.5 (m, 1H) 7.5 (dd, J=8.3, 1.7 Hz, 1H) 7.6 (m, 3H) 7.8 (d, J=8.3 Hz, 1H) 7.9 (m, 2H) 8.0 (dt, J=8.1, 1.1 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06875780B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-4b2d2484fca7450e92ef6dd927f295ec |
| Source note | uspto-grants-2005_04 |