4-Chlorobenzophenone → HCID 22505815, compound

HRID 1814206Notes

Reaction equation

HRID 1814206 reaction equation
P(Cl)(Cl)(Cl)(Cl)[Cl:2].[Cl:7][C:8]1[CH:21]=[CH:20][C:11]([C:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:13])=[CH:10][CH:9]=1>>[Cl-:2].[Cl-:7].[Cl:7][C:8]1[CH:9]=[CH:10][C:11]([C:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:13])=[CH:20][CH:21]=1

Participants

3

Reactant 2

HCID 86534-ChlorobenzophenoneHCID 24819Phosphorus pentachloride

Product 1

HCID 22505815HCID 22505815, compoundYield 89%

Procedure

The reaction was proceeded by the method described in Example 1. 21.6G of PCl5 was reacted with 20.8 g of 4-chlorobenzophenone to give 24.6 g(purity 98%, yield 89%) of 4-chlorobenzophenone dichloride as a colorless liquid.

Sources & evidence

ORD record
ord-67ba8519a7d14fd38c3dc30a5d62eb07
Source dataset
uspto-grants-2005_04
Patent number
US06875822B2

Reaction notes

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