4-Methylbenzophenone → HCID 22505813, compound

HRID 1814207Notes

Reaction equation

HRID 1814207 reaction equation
P(Cl)(Cl)(Cl)(Cl)[Cl:2].[CH3:7][C:8]1[CH:21]=[CH:20][C:11]([C:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:13])=[CH:10][CH:9]=1>>[Cl-:2].[Cl-:2].[CH3:7][C:8]1[CH:21]=[CH:20][C:11]([C:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:13])=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 86524-MethylbenzophenoneHCID 24819Phosphorus pentachloride

Product 1

HCID 22505813HCID 22505813, compoundYield 79%

Procedure

The reaction was proceeded by the method described in Example 1. 20.8G of PCl5 was reacted with 19.6 g of 4-methylbenzophenone to give 22.9 g(purity 87%, yield 79%) of 4-methylbenzophenone dichloride as a pale yellow liquid.

Sources & evidence

ORD record
ord-ed8a71e465a7443eaa9ea2cef9f8ae5b
Source dataset
uspto-grants-2005_04
Patent number
US06875822B2

Reaction notes

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