Phosphorus pentachloride → HCID 22505812, compound

HRID 1814208Notes

Reaction equation

HRID 1814208 reaction equation
P(Cl)(Cl)(Cl)(Cl)[Cl:2].[CH3:7][O:8][C:9]1[CH:22]=[CH:21][C:12]([C:13]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[O:14])=[CH:11][CH:10]=1>>[Cl-:2].[Cl-:2].[CH3:7][O:8][C:9]1[CH:22]=[CH:21][C:12]([C:13]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[O:14])=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 24819Phosphorus pentachlorideHCID 691464-Methoxybenzophenone

Product 1

HCID 22505812HCID 22505812, compoundYield 70%

Procedure

The reaction was proceeded by the method described in Example 1. 10.4G of PCl5 was reacted with 10.6 g of 4-methoxybenzophenone to give 10.6 g(purity 89%, yield 70%) of 4-methoxybenzophenone dichloride as a tan liquid.

Sources & evidence

ORD record
ord-67af6e1f7cb84e78b8685c8d38cf8364
Source dataset
uspto-grants-2005_04
Patent number
US06875822B2

Reaction notes

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