HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxide (P4O10) → 2,4-Dimethoxybenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxide (P4O10) | HCID 14812 | — |
| Reactant | 2,4-Dimethoxybenzaldoxime | HCID 231242 | — |
| Product | 2,4-Dimethoxybenzonitrile | HCID 77750 | — |
Reaction Steps
2,4-Dimethoxybenzoic acid is reacted with hydroxylamine to form 2,4-dimethoxybenzaldoxime. 2,4-Dimethoxybenzaldoxime is reacted with diphosphorus pentoxide to form 2,4-dimethoxybenzonitrile. 2,4-Dimethoxybenzonitrile is reacted with boron trichloride to form 2,4-dihydroxybenzonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06875883B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-67a8858791f4420992dbe1cb9d6ef1f8 |
| Source note | uspto-grants-2005_04 |