HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzaldehyde → HCID 9826552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzaldehyde | HCID 6996 | — |
| Reactant | 1-Phenylpiperazine | HCID 7096 | — |
| Reactant | 2-Thiocresol | HCID 8712 | — |
| Reactant | 6-Amino-1-hexanol | HCID 19960 | — |
| Reactant | 2,4-Dichlorobenzenethiol | HCID 70730 | — |
| Reactant | 4-Fluoro-3-(trifluoromethyl)benzaldehyde | HCID 522269 | — |
| Product | HCID 9826552 | HCID 9826552 | — |
Reaction Steps
The title compound was prepared by the procedures described in Example 1 substituting 2,4-dichlorothiophenol with 2-methylthiophenol, 2-chlorobenzaldehyde with 4fluoro-3-trifluoromethyl benzaldehyde, and 6-amino-1-hexanol with 4-phenylpiperazine. 1H NMR (CDCl3, 300 MHz) δ 7.81 (s, 1H); 7.64 (d, J=16.0 Hz, 1H); 7.51 (d, J=8.2 Hz, 1H); 7.40-7.27 (m, 6H); 6.98-6.90 (m, 4H); 6.80 (d, J=8.2 Hz, 1H); 3.88 (br s, 4H); 2.23 (br s, 4H); 2.34 (s, 3H). MS (ESI) m/z 987 (2M+Na)+, 965 (2M+H)+, 505 (M+Na)+, 483 (M+H)+, 451.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06878700B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-beeffade65d44fe6b3e5bfad04187ee1 |
| Source note | uspto-grants-2005_04 |