HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4-chlorophenol → 7-Bromo-5-chloro-1-benzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4-chlorophenol | HCID 69670 | — |
| Reactant | 2-(2-Bromo-4-chlorophenoxy)-acetaldehyde diethyl acetal | HCID 22144797 | — |
| Product | 7-Bromo-5-chloro-1-benzofuran | HCID 22144720 | — |
Reaction Steps
Beginning with 25 gm (120.5 mMol) 2-bromo-4-chlorophenol, 41.16 gm crude 2-(2-bromo-4-chlorophenoxy)acetaldehyde diethyl acetal was prepared essentially as described in Preparation IV. A sample of this crude material was subjected to silica gel chromatography to provide an analytical sample.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06881733B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-612337b5a5674dec9b2e26dbf0627e4b |
| Source note | uspto-grants-2005_04 |