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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1815846Generated: November 2, 2026

Hydrochloric Acid → HCID 69745334, compound

https://huagongshe.com/reaction/1815846

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 69745095HCID 69745095—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 69745334HCID 6974533496%

Reaction Steps

A mixture of 0.30 gm cis-1-(tert-butoxycarbonyl)-3-methyl-4-(5-methoxybenzofur-7-yl)piperidine in 10 mL 4N hydrochloric acid in dioxane is stirred at room temperature for 1 hour. The reaction mixture is concentrated under reduced pressure and the white solid residue is dried under reduced pressure at 60° C. for about 16 hours to provide 0.16 gm (96%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06881733B1
Source datasetuspto-grants-2005_04
ORD IDord-ba308e3f7b324e1aac6b5e6190778cfe
Source noteuspto-grants-2005_04