HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributylstannane → HCID 69744940, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributylstannane | HCID 5948 | — |
| Reactant | HCID 22495689 | HCID 22495689 | — |
| Product | HCID 69744940 | HCID 69744940 | 46.8% |
Reaction Steps
Beginning with 1.07 gm (2.33 mMol) 1-benzyl-3-methyl-4-(methyl oxoacetoxy)-4-(5-chloro-6-fluorobenzofur-7-yl)piperidine, this material was treated with tri(n-butyl)tin hydride essentially as described in EXAMPLE 16 to provide 0.39 gm of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06881733B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-2e4b5cc4194e443a930cc741b3a8fa0b |
| Source note | uspto-grants-2005_04 |