huagongshe.com
HRID1815968

反应详情

EQUATION

反应方程式

HRID 1815968 的结构方程式

REACTANTS

反应物

1
结构：C[C@@H](Cn1ncc2ccc3c(c21)CC(O)CO3)N=[N+]=[N-]
HCID86759652

未命名化合物

PRODUCTS

生成物

1
结构：C[C@H](N)Cn1ncc2ccc3c(c21)CC(O)CO3
HCID9834763

未命名化合物

收率 88%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of the product from Step A in methanol was treated as described in Example 2, Step J to give the free base as an amorphous solid (0.36 g, 88%): mp 46-51° C.; GCMS(Cl+) m/z 248 (M+H). Analysis. Calculated for C13H17N3O2.0.1H2O: C, 62.68; H, 6.96; N, 16.97. Found: C, 62.55; H, 7.03; N, 16.64.