HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Isopropylethylenediamine → 2-Chloro-5-[[[2-[(1-methylethyl)amino]ethyl]amino]methyl]-N-(tricycio[3.3.1.13,7]dec-1-ylmethyl)-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Isopropylethylenediamine | HCID 88098 | — |
| Reactant | 2-Chloro-5-formyl-N-(tricyclo [3.3.1.13,7]dec-1-ylmethyl)-benzamide | HCID 12085346 | — |
| Product | 2-Chloro-5-[[[2-[(1-methylethyl)amino]ethyl]amino]methyl]-N-(tricycio[3.3.1.13,7]dec-1-ylmethyl)-benzamide | HCID 10136764 | 16.7% |
Reaction Steps
Synthesised as in Example 26 using 2-chloro-5-formyl-N-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamide (0.500 g, Example 25b) and N-isopropylethylenediamine (0.186 g) to give the title compound as a solid (0.105 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06881754B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-cb013198c1b3466ba8643e9dd74bc77c |
| Source note | uspto-grants-2005_04 |