3-Cyclohexene-1-carboxylic acid → Cyclohexanecarboxylic acid

HRID 1816085Notes

Reaction equation

HRID 1816085 reaction equation
[CH:1]1([C:7]([OH:9])=[O:8])[CH2:6][CH2:5][CH:4]=[CH:3][CH2:2]1.[H][H]>[Pd]>[CH:1]1([C:7]([OH:9])=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 209033-Cyclohexene-1-carboxylic acidHCID 178418361HCID 178418361, compound

Product 1

HCID 7413Cyclohexanecarboxylic acid

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

3.2 g (2.5 wt. % of 3-cyclohexene-1-carboxylic acid) 3% Pd/C was added to the 3-cyclohexene-1-carboxylic acid solution and the reaction was activated at the temperature of 100° C. with a hydrogen pressure of 120 psi to yield cyclohexanecarboxylic acid with a conversion rate of more than 99%.

Sources & evidence

ORD record
ord-8e23f0dc6a18427199a5279e5c04f2a1
Source dataset
uspto-grants-2005_04
Patent number
US06881865B2

Reaction notes

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