HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86592292, compound → HCID 22492617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86592292 | HCID 86592292 | — |
| Reactant | HCID 178418806 | HCID 178418806 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 22492617 | HCID 22492617 | — |
Reaction Steps
2.5 g (7.6 mmol) of 2-(4-methoxyphenylazo)-1,3-dimethyl-3H-imidazol-1-ium perchlorate and 50 ml of 2-propanol are charged to a fully equipped round-bottomed flask. The mixture is brought to 60° C. 1.3 g (15.5 mmol) of 3-aminopyrazole are added. This mixture is brought, with stirring, to the reflux temperature of the solvent for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06884267B2 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-a718550a68d44821be2ec5db6986f1de |
| Source note | uspto-grants-2005_04 |