HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-nitrobenzene → HCID 15588201, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-nitrobenzene | HCID 11341 | — |
| Reactant | 1-Methyl-2-(trimethylstannyl)-1H-pyrrole | HCID 13664967 | — |
| Product | HCID 15588201 | HCID 15588201 | 68.6% |
Reaction Steps
1-Methyl-2-(trimethylstannyl)-1H-pyrrole (3.94 g, 14.7 mmol) and 1-bromo-2-nitrobenzene (3.22 g, 15.9 mmol, 1.08 eq) were coupled as in Example 75 to give 2.04 g of 1-methyl-2-(2-nitrophenyl)-1H-pyrrole, which was reduced as in Example 64 to give 1.53 g of 2-(1-methyl-1H-pyrrol-2-yl)aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06884801B1 |
| Source dataset | uspto-grants-2005_04 |
| ORD ID | ord-6332f2f6c2934a0a965c535136463f42 |
| Source note | uspto-grants-2005_04 |