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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1816610Generated: October 31, 2026

HCID 22494136, compound → HCID 22494177, compound

https://huagongshe.com/reaction/1816610

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22494136HCID 22494136—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 22494177HCID 2249417792.6%

Reaction Steps

29 mg of ethyl 3-(7-[(tertiary butoxycarbonyl)amino]methylbenzo[b]furan-5-yl)-2-isopropoxypropionate was dissolved in ethanol, and 30 mg of 10% palladium-carbon was added, and the mixture was stirred at room temperature for 3 days in a hydrogen atmosphere. The reaction mixture was filtered through Celite, and the filtrate was concentrated, to give 27 mg of ethyl 3-(7-[(tertiary butoxycarbonyl)amino]methyl-2,3-dihydrobenzo[b]furan-5-yl)-2-isopropoxypropionate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06884821B1
Source datasetuspto-grants-2005_04
ORD IDord-fd29410ab9d049b0a2916f1f776ab779
Source noteuspto-grants-2005_04