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HRID1816880

反应详情

EQUATION

反应方程式

HRID 1816880 的结构方程式

REACTANTS

反应物

2
反应SMILES：O=C=NS(=O)(=O)Cl
HCID70918

Sulfuryl chloride isocyanate

CClNO3S

反应SMILES：CC(C)(C)OC(=O)n1cccc1-c1ccc2c(c1)C(C)(C)OCC(=O)N2
HCID68866427

未命名化合物

PRODUCTS

产物

1
反应SMILES：CC(C)(C)OC(=O)n1c(C#N)ccc1-c1ccc2c(c1)C(C)(C)OCC(=O)N2
HCID24956378

未命名化合物

PROCEDURE

实验过程

Prepared from tert-butyl-2-(5,5-dimethyl-2-oxo-1,2,3,5-tetrahydro-4,1-benzoxazepin-7-yl)-1H-pyrrole-1-carboxylate and chlorosulfonyl isocyanate generally according to the procedure described in example 1. 1H-NMR (DMSO-d6) δ 10.03 (s, 1H), 7.35 (d, J=1.79 Hz, 1H), 7.31 (d, J=3.8 Hz, 1H), 7.23 (dd, J=1.79, 8.31 Hz, 1H), 7.12 (d, J=8.36 Hz, 1H), 6.44 (d, J=3.81 Hz, 1H), 4.25 (s, 2H), 1.55 (s, 6H), 1.39 (s, 9H).