HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzylpiperidine → 4-benzyl-N-(4-methylphenyl)piperidine-1-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzylpiperidine | HCID 31738 | — |
| Reactant | 4-Biphenylyl isocyanate | HCID 3612319 | — |
| Product | 4-benzyl-N-(4-methylphenyl)piperidine-1-carboxamide | HCID 1836814 | — |
Reaction Steps
The title compound was prepared from 4-benzylpiperidine and 4-phenylphenyl isocyanate. 1H NMR (400 MHz, CDCl3): 7.31-7.12 (m, 7H), 7.07 (d, J=8.0 Hz, 2H), 6.32 (s, 1H), 4.06-4.00 (m, 2H), 2.79 (td, J=13, 2.5 Hz, 2H), 2.56 (d, J=6.8 Hz, 2H), 2.28 (s, 3H), 1.79-0.165 (m, 3H), 1.30-1.18 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598249B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-1524b5829fbc46dd80f035fac459dbbd |
| Source note | uspto-grants-2009_10 |