HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzylpiperidine → 4-Benzyl-piperidine-1-carboxylic acid m-tolylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzylpiperidine | HCID 31738 | — |
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Product | 4-Benzyl-piperidine-1-carboxylic acid m-tolylamide | HCID 3833631 | — |
Reaction Steps
The title compound was prepared from 4-benzylpiperidine and 3-methylphenyl isocyanate. 1H NMR (400 MHz, CDCl3): 7.32-7.07 (m, 8H), 6.84-6.80 (m, 1H), 6.41 (br s, 1H), 4.06-4.00 (m, 2H), 2.78 (td, J=13 Hz, 2.4 Hz, 2H), 2.55 (d, J=7.0 Hz, 2H), 2.30 (s, 3H), 1.77-1.64 (m, 3H), 1.28-1.16 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598249B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-a0a8288463314e33acf4b8f53bd3a852 |
| Source note | uspto-grants-2009_10 |