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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1817097Generated: October 26, 2026

3-Iodobenzaldehyde → 4-(3-Iodo-benzyl)-piperazine-1-carboxylic acid phenylamide

https://huagongshe.com/reaction/1817097

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-IodobenzaldehydeHCID 252610—
ReactantN-phenylpiperazine-1-carboxamideHCID 7015289—
Product4-(3-Iodo-benzyl)-piperazine-1-carboxylic acid phenylamideHCID 24020419—

Reaction Steps

The title compound was prepared from piperazine-1-carboxylic acid phenylamide and 3-iodobenzaldehyde. 1H NMR (400 MHz, CDCl3): 7.71 (s, 1H), 7.62-7.60 (m, 1H), 7.36-7.26 (m, 5H), 7.09-7.01 (m, 2H), 6.33 (s, 1H), 3.52-3.48 (m, 6H), 2.49-2.46 (m, 4H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07598249B2
Source datasetuspto-grants-2009_10
ORD IDord-68452dbc46a94a9d97da663428466f1a
Source noteuspto-grants-2009_10