HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonal → 4-(1,3-benzodioxol-5-ylmethyl)-N-(4-fluorophenyl)piperazine-1-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonal | HCID 8438 | — |
| Reactant | N-(4-Fluorophenyl)piperazine-1-carboxamide | HCID 16228149 | — |
| Product | 4-(1,3-benzodioxol-5-ylmethyl)-N-(4-fluorophenyl)piperazine-1-carboxamide | HCID 1079407 | — |
Reaction Steps
The title compound was prepared from piperazine-1-carboxylic acid (4-fluoro-phenyl)-amide and piperonal. 1H NMR (400 MHz, CDCl3): 7.29-7.24 (m, 2H), 6.98-6.92 (m, 2H), 6.85 (s, 1H), 6.77-6.71 (m, 2H), 6.56 (s, 1H), 5.95 (s, 2H), 3.50-3.45 (m, 6H), 2.45 (t, J=5.1 Hz, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598249B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-0efec55d77784a8c90804dce228735db |
| Source note | uspto-grants-2009_10 |