HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-2-tetralone → 4-(6-Bromo-1,2,3,4-tetrahydro-naphthalen-2-yl)-piperazine-1-carboxylic acid phenylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-2-tetralone | HCID 2733553 | — |
| Reactant | N-phenylpiperazine-1-carboxamide | HCID 7015289 | — |
| Product | 4-(6-Bromo-1,2,3,4-tetrahydro-naphthalen-2-yl)-piperazine-1-carboxylic acid phenylamide | HCID 57880869 | — |
Reaction Steps
The title compound was prepared from piperazine-1-carboxylic acid phenylamide and 6-bromo-3,4-dihydro-1H-naphthalen-2-one. 1H NMR (400 MHz, CDCl3): 7.37-7.21 (m, 6H), 7.06-7.02 (m, 1H), 6.96-6.94 (m, 1H), 6.33 (s, 1H), 3.55-3.53 (m, 4H), 2.94-2.64 (m, 9H), 2.12-2.08 (m, 1H), 1.69-1.61 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598249B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-7620dd1303f948ab8d0bf951dcb9ad6d |
| Source note | uspto-grants-2009_10 |