HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoromethanesulfonyl chloride → HCID 86598624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoromethanesulfonyl chloride | HCID 79000 | — |
| Reactant | HCID 67401517 | HCID 67401517 | — |
| Product | HCID 86598624 | HCID 86598624 | 59.9% |
Reaction Steps
A solution of trifluoromethanesulfonyl chloride (10 mmol) and (E)-2,4,6-trimethoxystyryl-3-amino-4-methoxybenzylsulfone (10 mmol) was reacted according to General Method A. The product obtained was purified by column chromatography to give the desired product in 59.9% yield. (m.p. 144-46° C.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598232B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-05d4437f244a46d9aa7cd1063777daf1 |
| Source note | uspto-grants-2009_10 |