HRID1817148

反应详情

EQUATION

反应方程式

HRID 1817148 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Ethyl-(3-nitropyridin-4-yl)amine (8.7 g, 52.0 mmol) in ethanol (150 ml) was hydrogenated for 18 hours in the presence of 10% palladium on carbon. After filtration of the catalyst through celite, the filtrate was concentrated in vacuo to afford the title compound (6.7 g, 94%).

WORKUP

后处理

  1. filtrationAfter filtration of the catalyst through celite
  2. concentrationthe filtrate was concentrated in vacuo