HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-1-propanol → HCID 11676571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-1-propanol | HCID 12308 | — |
| Reactant | HCID 11716432 | HCID 11716432 | — |
| Product | HCID 11676571 | HCID 11676571 | 64.9% |
Reaction Steps
Following the general procedure outlined in Example 7, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)acetonitrile (0.0495 g, 0.164 mmol) and 3-bromo-1-propanol (0.030 mL, 0.343 mmol) in 2CH3CN/3CHCl3 (4.0 mL) were reacted to give the desired product (0.0467 g, 64.9%). EI-MS m/z 361 (M+) Rt (1.98 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598267B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-e0ccf91c6bee45eca9bdd63031935ccc |
| Source note | uspto-grants-2009_10 |