Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Ethylpiperazine | HCID 79196 | — |
| Reactant | Dinitrobenzonitrile | HCID 520718 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22664750 | HCID 22664750 | — |
Reaction Steps
2,6-Dinitrobenzenecarbonitrile (1.0 eq) and ethylpiperazine (3.6 eq) were dissolved in DMF. The resulting solution heated at 90° C. for 2 hours. The solution was cooled to room temperature and poured into H2O. A precipitate formed which was filtered to yield the desired product as a brown solid. LC/MS m/z 260.1 (MH+), Rt 1.69 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07598268B2 |
|---|
| Source dataset | uspto-grants-2009_10 |
|---|
| ORD ID | ord-8ebc618d13a54bb994bc519d7de0157f |
|---|
| Source note | uspto-grants-2009_10 |
|---|
