HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 9878038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 67190505 | HCID 67190505 | — |
| Catalyst | HCID 178506449 | HCID 178506449 | — |
| Product | HCID 9878038 | HCID 9878038 | 60% |
Reaction Steps
Ethyl p-nitro-2-ethoxycinnamate obtained in step (i) was hydrogenated using 10% Pd—C—H2 (60 psi) (11 g) in ethyl acetate (150 mL) at room temperature and chromatographed using ethyl acetate/hexane to yield the title compound as viscous oil (9.41 g, 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598293B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-e22275e4e1804ba3953bba8fb9895f42 |
| Source note | uspto-grants-2009_10 |