tert-Butyl mercaptan → HCID 68870468, compound

HRID 1817880Notes

Reaction equation

HRID 1817880 reaction equation
[C:1]([C:5]1[N:9]([CH2:10][CH:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)[C:8]2[CH:17]=[CH:18][C:19]([CH2:21]Cl)=[CH:20][C:7]=2[N:6]=1)([CH3:4])([CH3:3])[CH3:2].[CH3:23][C:24]([SH:27])([CH3:26])[CH3:25]>>[C:1]([C:5]1[N:9]([CH2:10][CH:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)[C:8]2[CH:17]=[CH:18][C:19]([CH2:21][S:27][C:24]([CH3:26])([CH3:25])[CH3:23])=[CH:20][C:7]=2[N:6]=1)([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 6387tert-Butyl mercaptanHCID 68872674HCID 68872674, compound

Product 1

HCID 68870468HCID 68870468, compound

Procedure

The title compound was prepared according to the procedure described in step F of Example 15 from 2-tert-butyl-5-(chloromethyl)-1-(tetrahydro-2H-pyran-4-ylmethyl)-1H-benzimidazole (step F of Example 25) and 2-methyl-2-propanethiol.

Sources & evidence

ORD record
ord-e488addd63d94dbebe87d199d9da4a1b
Source dataset
uspto-grants-2009_10
Patent number
US07598393B2

Reaction notes

Loading…