Ethanethiol → HCID 68873560, compound

HRID 1817910Notes

Reaction equation

Br[C:2]1[CH:3]=[C:4]2[N:10]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[N:8]([CH2:15][CH:16]3[CH2:21][CH2:20][O:19][CH2:18][CH2:17]3)[C:5]2=[N:6][CH:7]=1.[CH2:22]([SH:24])[CH3:23]>>[C:11]([C:9]1[N:8]([CH2:15][CH:16]2[CH2:21][CH2:20][O:19][CH2:18][CH2:17]2)[C:5]2=[N:6][CH:7]=[C:2]([S:24][CH2:22][CH3:23])[CH:3]=[C:4]2[N:10]=1)([CH3:14])([CH3:13])[CH3:12]

Participants

Reactant 2

HCID 6343Ethanethiol

HCID 68872524HCID 68872524, compound

Product 1

HCID 68873560HCID 68873560, compound

Procedure

The title compound was prepared according to the procedure described in Step E of Example 32 from 6-bromo-2-tert-butyl-3-(tetrahydro-2H-pyran-4-ylmethyl)-3H-imidazo[4,5-b]pyridine (Step F) and ethanethiol (Wako Pure Chemical Industries, Ltd.).

Sources & evidence

ORD record: ord-8a2ded7b685043cea7a93287f1b1e352
Source dataset: uspto-grants-2009_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07598393B2

Reaction notes

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