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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1818031Generated: October 31, 2026

Beta-Alanine → HCID 10222358, compound

https://huagongshe.com/reaction/1818031

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBeta-AlanineHCID 239—
ReactantWaterHCID 962—
Reactant2-Propenal, 3-(4-hydroxy-3,5-dimethoxyphenyl)-HCID 119216—
ReactantHCID 86760966HCID 86760966—
SolventEthanolHCID 702—
ProductHCID 10222358HCID 1022235875%

Reaction Steps

To 3,5-dimethoxy-4-hydroxycinnamaldehyde (0.042 g, 0.2 mmol) and N-cyanoacetyl)3,4-dihydroxybenzylamide (Example 2, 0.042 g, 0.2 mmol) in 10 ml of ethanol 3 mg of β-alanine was added and the reaction was refluxed for 6 h. Water was added and the solid was recrystallized from 5 ml of ethanol twice to give 0.06 g (75%) of a red solid. The product gave the following analytical data:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07598419B2
Source datasetuspto-grants-2009_10
ORD IDord-7456f67ff3c5420782bda42e1af6f664
Source noteuspto-grants-2009_10