HuagongsheHuagongshe Chemistry Print Report · For research reference only
Beta-Alanine → HCID 10222358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Beta-Alanine | HCID 239 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Propenal, 3-(4-hydroxy-3,5-dimethoxyphenyl)- | HCID 119216 | — |
| Reactant | HCID 86760966 | HCID 86760966 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10222358 | HCID 10222358 | 75% |
Reaction Steps
To 3,5-dimethoxy-4-hydroxycinnamaldehyde (0.042 g, 0.2 mmol) and N-cyanoacetyl)3,4-dihydroxybenzylamide (Example 2, 0.042 g, 0.2 mmol) in 10 ml of ethanol 3 mg of β-alanine was added and the reaction was refluxed for 6 h. Water was added and the solid was recrystallized from 5 ml of ethanol twice to give 0.06 g (75%) of a red solid. The product gave the following analytical data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598419B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-7456f67ff3c5420782bda42e1af6f664 |
| Source note | uspto-grants-2009_10 |