HRID1818033
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The compound was prepared as described in Example 3, by adding 3,4-dimethoxycinnamaldehyde (Example 6, 0.04 g, 0.2 mmol) to N-(cyanoacetyl)benzylamide (Example 4, 0.036 g, 0.2 mmol). After refluxing for 1 h and recrystallization from ethanol a yellow solid was obtained (0.045 g, 62%). The product gave the following analytical data:
WORKUP
后处理
- customThe compound was prepared
- temperatureAfter refluxing for 1 h
- customrecrystallization from ethanol a yellow solid
- customwas obtained (0.045 g, 62%)
- customThe product gave the following analytical data