HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl cyanoacetate → HCID 9900601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl cyanoacetate | HCID 7747 | — |
| Reactant | 2-Propenal, 3-(4-hydroxy-3,5-dimethoxyphenyl)- | HCID 119216 | — |
| Product | HCID 9900601 | HCID 9900601 | — |
Reaction Steps
The compound was prepared as described in Example 3 by adding 3,5-dimethoxy-4-hydroxycinnamaldehyde (0.15 g, 0.72 mmol) to methyl cyanoacetate (0.064 ml, 0.72 mmol). After refluxing for 1 h and recrystallization from ethanol an orange solid was obtained (0.2 g, 90%). The product gave the following analytical data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598419B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-66e4f36731cd421da500bedef4c70b75 |
| Source note | uspto-grants-2009_10 |