HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 11500983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 3-(3,4-Dihydroxy-phenyl)-2-propenal | HCID 443034 | — |
| Reactant | 2-cyano-N-[(3-fluorophenyl)methyl]acetamide | HCID 28970880 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11500983 | HCID 11500983 | — |
Reaction Steps
The compound was prepared as described in Example 37 by adding piperidine to a solution of 3,4-dihydroxycinnamaldehyde (35 mg, 0.2 mmol) and 2-cyano-N-(3-fluorobenzyl)acetamide (38 mg, 0.2 mmol) in ethanol. After recrystallization from ethanol-water a yellow solid was obtained (51 mg, 75%). The product gave the following analytical data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598419B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-8b4890e42bc4430b84d5f68d83900e42 |
| Source note | uspto-grants-2009_10 |