HRID1818048
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The compound was prepared as described in Example 3 by adding 3,4-dihydroxycinnamaldehyde (32 mg, 0.2 mmol) to 2-cyano-N-pyridin-4-ylmethylacetamide (33 mg, 0.2 mmol). After refluxing for 2 h and recrystallization from ethanol-water an orange solid was obtained (44 mg, 69%). The product gave the following analytical data:
WORKUP
后处理
- customThe compound was prepared
- temperatureAfter refluxing for 2 h
- customrecrystallization from ethanol-water an orange solid
- customwas obtained (44 mg, 69%)
- customThe product gave the following analytical data