HRID1818048

反应详情

EQUATION

反应方程式

HRID 1818048 的结构方程式

PROCEDURE

实验过程

The compound was prepared as described in Example 3 by adding 3,4-dihydroxycinnamaldehyde (32 mg, 0.2 mmol) to 2-cyano-N-pyridin-4-ylmethylacetamide (33 mg, 0.2 mmol). After refluxing for 2 h and recrystallization from ethanol-water an orange solid was obtained (44 mg, 69%). The product gave the following analytical data:

WORKUP

后处理

  1. customThe compound was prepared
  2. temperatureAfter refluxing for 2 h
  3. customrecrystallization from ethanol-water an orange solid
  4. customwas obtained (44 mg, 69%)
  5. customThe product gave the following analytical data