HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Methylthio)propylamine → (3-Methylsulfanylpropyl)-(3-nitro-7-phenylquinolin-4-yl)amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Methylthio)propylamine | HCID 77743 | — |
| Reactant | 4-Chloro-3-nitro-7-phenylquinoline | HCID 21984335 | — |
| Product | (3-Methylsulfanylpropyl)-(3-nitro-7-phenylquinolin-4-yl)amine | HCID 21984176 | 93.3% |
Reaction Steps
4-Chloro-3-nitro-7-phenylquinoline (5.3 g, 18.8 mmol) and 3-methylsulfanyl-propylamine (2.17 g, 20.6 mmol) were combined and treated according to the general procedure described in Part E of Example 1. Recrystallization from isopropanol afforded 6.2 g of (3-methylsulfanylpropyl)-(3-nitro-7-phenylquinolin-4-yl)amine as gold plates.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598382B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-280e436433df4fab90668d8bcd70c856 |
| Source note | uspto-grants-2009_10 |