HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxypropylamine → (7-Bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxypropylamine | HCID 1672 | — |
| Reactant | 7-Bromo-4-chloro-3-nitroquinoline | HCID 21984361 | — |
| Product | (7-Bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine | HCID 21984327 | 94.2% |
Reaction Steps
7-Bromo-4-chloro-3-nitroquinoline (29.54 g, 102.7 mmol) was reacted with 3-methoxy propyl amine (10.07 g, 113.0 mmol) according to the method described in Part A of Examples 125-135 to provide 32.9 g of (7-bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine as a yellow solid. The product was not recrystallized.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598382B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-0577e3a026534b0f825b9a02214d4dce |
| Source note | uspto-grants-2009_10 |