HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → 7-Benzyl-4-chloro-3-nitroquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178418731 | HCID 178418731 | — |
| Reactant | HCID 178418920 | HCID 178418920 | — |
| Product | 7-Benzyl-4-chloro-3-nitroquinoline | HCID 21984193 | — |
| Product | 6-Benzyl-4-chloro-3-nitroquinoline | HCID 21984226 | — |
Reaction Steps
The method described in Part E of Example 10 was used to treat 7-benzyl-3-nitroquinolin-4-ol or 6-benzyl-3-nitroquinolin-4-ol with phosphorous oxychloride to provide 7-benzyl-4-chloro-3-nitroquinoline as a light yellow powder or 6-benzyl-4-chloro-3-nitroquinoline as a tan powder, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07598382B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-d9aa6157ee124163acca2e2d1cb9658f |
| Source note | uspto-grants-2009_10 |