Oxalyl chloride → HCID 10869449, compound

Participants

Reaction Steps

Synthesis of MC810 (FIG. 7). To a solution of palmitoleic acid (cis-9-hexadecanoic acid, 2.00 g, 7.87 mmol, Aldrich Chemical Company) in dichloromethane (75 mL), was added oxalyl chloride (1.72 mL, 19.7 mmol, Aldrich Chemical Company) dropwise under nitrogen. After 16 hrs, the solution was concentrated under reduced pressure (aspirator) and then placed under high vacuum to afford palmitoleoyl chloride.

Provenance & Evidence