HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethylpiperazine → HCID 57886308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethylpiperazine | HCID 66056 | — |
| Reactant | HCID 68713669 | HCID 68713669 | — |
| Product | HCID 57886308 | HCID 57886308 | 99.5% |
Reaction Steps
In an analogous manner as described in general procedure V, 1-(5-bromopentyl)-3-(2-fluorophenyl)-1,3-dihydro-2,1,3-benzothiadiazole 2,2-dioxide (0.07 g, 0.18 mmol) was treated with 2,6-Dimethyl-piperazine (0.06 g, 0.54 mmol) to provide 0.08 g (88%) of 1-[5-(3,5-dimethylpiperazin-1-yl)pentyl]-3-(2-fluorophenyl)-1,3-dihydro-2,1,3-benzothiadiazole 2,2-dioxide. MS (ES) m/z 447.0;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601722B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-ecb97ed4d34741abb805a744c9ce979c |
| Source note | uspto-grants-2009_10 |