HCID 23119185, compound → HCID 23119404, compound

Participants

Reaction Steps

To a THF (60 mL) solution of 5-(3-methyloxyhexyn-1-yl)tetralone (5) (11 g) was added 10% palladium-carbon (0.9 g), and the reaction mixture was stirred under a hydrogen gas atmosphere for 5 h. The reaction mixture filtered off, and the filtrate was evaporated. The obtained residue was purified by column chromatography (hexane:ethyl acetate=9:1) to obtain the compoumd (6) 9.0 g.

Provenance & Evidence