Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Methylindole | HCID 7224 | — |
| Reactant | HCID 67316943 | HCID 67316943 | — |
| Product | HCID 67315836 | HCID 67315836 | — |
Reaction Steps
The product of example 22, step b) (230 mg, 0.89 mmol) was treated with 2-methyl indole (196 mg, 1.5 mmol) and heated (neat) to 180° C. for 1 h. The reaction was cooled and the sub-title product was purified by silica chromatography (EtOAc/Hex).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07601749B2 |
|---|
| Source dataset | uspto-grants-2009_10 |
|---|
| ORD ID | ord-3b16b7b0bf4742a9b22baad9e6031036 |
|---|
| Source note | uspto-grants-2009_10 |
|---|
