HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[1-(4-fluorobenzyl)-1H-indol-3-yl]acetic acid → HCID 178512406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[1-(4-fluorobenzyl)-1H-indol-3-yl]acetic acid | HCID 2774436 | — |
| Reactant | 4-Amino-3,5-dichlorobenzylamine | HCID 18975763 | — |
| Reactant | HCID 178488081 | HCID 178488081 | — |
| Product | HCID 178512406 | HCID 178512406 | — |
Reaction Steps
In a manner similar to that used in the preparation of the compound of example 2, but using 2-(1-(4-fluorobenzyl)-1H-indol-3-yl)acetic acid in step 6 (A) and 3,5-dichloro-4-aminobenzylamine (preparation A) in step 6 (B), the title compound was prepared. MS (ESI) (M+H)+=498.08 1H-NMR(500 MHz, CD3OD) δ 7.58 (d, J=7.63 Hz, 1 H), 7.26-7.40 (m, 2 H), 7.13-7.25 (m, 5 H), 7.05-7.13 (m, 1 H), 7.01 (t, J=8.70 Hz, 2 H), 5.33 (s, 2 H), 4.32 (s, 2 H), 3.96 (s, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601751B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-b5725389db624e279fc8f15f71b8d853 |
| Source note | uspto-grants-2009_10 |