HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-3-indoleacetic acid → HCID 178512110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-3-indoleacetic acid | HCID 96734 | — |
| Reactant | 4-Amino-3,5-dichlorobenzylamine | HCID 18975763 | — |
| Reactant | HCID 178488081 | HCID 178488081 | — |
| Product | HCID 178512110 | HCID 178512110 | — |
Reaction Steps
In a manner similar to that used in the preparation of the compound of example 2, but using 2-(5-bromo-1H-indol-3-yl)acetic acid in step 17 (A) and 3,5-Dichloro-4-aminobenzylamine (preparation A) in step 17 (B), the title compound was prepared. MS (ESI) (M+H)+=467.90/469.86/471.83 1H-NMR (500 MHz, CD3OD) δ 7.71 (s, 1 H), 7.32 (m, 2 H), 7.16-7.28 (m, 3 H), 4.35 (s, 2 H), 3.93 (s, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601751B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-1e9feb3527c84cb3a23667ba63b8700e |
| Source note | uspto-grants-2009_10 |