HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-2,6-dichlorophenol → HCID 18511620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-2,6-dichlorophenol | HCID 80037 | — |
| Reactant | 2-Chloro-6-(trifluoromethoxy)-1,3-benzothiazole | HCID 10037924 | — |
| Product | HCID 18511620 | HCID 18511620 | — |
Reaction Steps
3,5-Dichloro-4-(6-trifluoromethoxy-benzothiazol-2-yloxy)-phenylamine was synthesized (76%) from 2-chloro-6-trifluoromethoxybenzotiazole (413) and 4-amino-2,6-dichlorophenol (Aldrich) in a similar manner as described in Example 417. 1H NMR (400 MHz, DMSO-d6) δ 8.10 (d, J=1.6 Hz, 1H), 7.80 (d, J=8.8 Hz, 1H), 7.44 (ddd, J=8.8, 1.6, 0.8 Hz, 1H), 6.74 (s, 2H), 5.87 (s, 2H). MS (EI): m/z 395 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601841B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-6ab06f10c0ec4a87807f9d8ceb5cea04 |
| Source note | uspto-grants-2009_10 |