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HRID1819813

反应详情

EQUATION

反应方程式

HRID 1819813 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1ccc(S(=O)(=O)Cl)cc1
HCID266418

4-Acetylbenzenesulfonyl chloride

C8H7ClO3S

结构：Nc1cc(Cl)c(Oc2nc3ccc(Cl)cc3s2)c(Cl)c1
HCID22148776

3,5-Dichloro-4-[(6-chloro-2-benzothiazolyl)oxy]benzenamine

C13H7Cl3N2OS

PRODUCTS

生成物

1
结构：CC(=O)c1ccc(S(=O)(=O)Nc2cc(Cl)c(Oc3nc4ccc(Cl)cc4s3)c(Cl)c2)cc1
HCID18511606

未命名化合物

PROCEDURE

实验过程

4-Acetyl-N-[3,5-dichloro-4-(6-chloro-benzothiazol-2-yloxy)-phenyl]-benzenesulfonamide was synthesized (36%) from 3,5-dichloro-4-(6-chloro-benzothiazol-2-yloxy)-phenylamine (420) and 4-acetyl-benzenesulfonyl chloride (Fluka) in a similar manner as described in Examples 70-91. 1H NMR (400 MHz, DMSO-d6) δ 11.24 (br s, 1H), 8.18 (dd, J=7.8, 1.7 Hz, 2H), 8.15 (d, J=2.2 Hz, 1H), 8.01 (d, J 7.8, 1.7 Hz, 2H), 7.67 (d, J=8.7 Hz, 1H), 7.46 (dd, J=8.7, 2.2 Hz, 1H), 7.32 (s, 2H), 2.63 (s, 3H). MS (EI): m/z 525 (M−H).