HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2E)-3-(2,4-Dimethoxy-3-phenylphenyl)prop-2-enoic acid → 3-(2,4-Dimethoxy-3-phenylphenyl)propanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2E)-3-(2,4-Dimethoxy-3-phenylphenyl)prop-2-enoic acid | HCID 21946110 | — |
| Reactant | 3-(3-Chloro-2,4-dimethoxyphenyl)propionic acid | HCID 21946112 | — |
| Product | 3-(2,4-Dimethoxy-3-phenylphenyl)propanoic acid | HCID 21946107 | 98% |
Reaction Steps
Compound 4c was synthesized from 3c in 98% yield using the procedure described for 4a. 1H NMR (DMSO-d6): δ 12.0 (br s, 1H), 7.39 (m, 2H), 7.29 (m, 3H), 7.18 (d, J=8.5 Hz, 1H), 6.80 (d, J=8.5 Hz, 1H), 3.64 (s, 3H), 3.18 (s, 3H), 2.78 (t, J=7.5 Hz, 2H), 2.50 (t, J=7.5 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601851B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-f5b8e0f008a14243a364d72ccb934358 |
| Source note | uspto-grants-2009_10 |