Triethylamine → HCID 24899193, compound

Participants

Reaction Steps

Following the procedure of Example 1, tetrahydro-dibenzofuran-2-ylamine (1.1 g, 6.0 mmol), t-butylacetyl chloride (0.93 mL, 6.6 mmol), and triethylamine (2.6 mL, 18 mmol) in tetrahydrofuran (11 mL) provided 3,3-dimethyl-N-(6,7,8,9-tetrahydro-dibenzofuran-2-yl)-butyramide (0.92 g). Mp 164-165° C.; Anal. Calcd. for C18H23NO2: C, 75.76; H, 8.12; N, 4.91; Found: C, 75.62; H, 8.18; N, 5.00.

Provenance & Evidence