4-Chlorobenzoyl chloride → HCID 24899702, compound

Participants

Reaction Steps

Following the procedure of Example 1, tetrahydro-dibenzofuran-2-ylamine (0.94 g, 5.0 mmol) and p-chlorobenzoyl chloride (0.72 mL, 5.5 mmol) in pyridine (10 mL) provided 4-chloro-N-(6,7,8,9-tetrahydro-dibenzofuran-2-yl)-benzamide (1.0 g). Mp 214.0-214.5° C.; Anal. Calcd. for C19H16CINO2: C, 70.05; H, 4.95; N, 4.30; Found: C, 70.10; H, 4.72; N, 4.17.

Provenance & Evidence