HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanoyl chloride → HCID 24899705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanoyl chloride | HCID 64801 | — |
| Reactant | HCID 21221605 | HCID 21221605 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 24899705 | HCID 24899705 | 50.9% |
Reaction Steps
Following the procedure of Example 1, tetrahydro-dibenzofuran-2-ylamine (0.15 g, 0.80 mmol), hydrocinnamoyl chloride (0.12 mL, 0.80 mmol), and poly(vinylpyridine) (0.5 g) in dichloroethane (8 mL) provided 3-phenyl-N-(6,7,8,9-tetrahydrodibenzo[b,d]furan-2-yl)propanamide (0.13 g) after flash column chromatography (elution with 35% ethyl acetate-hexanes). MS (ESI) m/z 320.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07601856B2 |
| Source dataset | uspto-grants-2009_10 |
| ORD ID | ord-1359cd3a4a144b2484fae6fc527bd95e |
| Source note | uspto-grants-2009_10 |